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Theses and Dissertations - Department of Metallurgical and Materials Engineering

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Browsing Theses and Dissertations - Department of Metallurgical and Materials Engineering by Author "Amaro, Robert L."

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    Advanced characterization of the oxidation behavior of grain refined NiAl
    (University of Alabama Libraries, 2019) White, Rachel Ellen; Weaver, Mark Lovell; University of Alabama Tuscaloosa
    Reactive element doped β-NiAl is one of the most oxidation resistant materials available for high temperature use. It has been extensively studied to create the most adherent, slow growing, and passive layer possible. One recent area of interest is grain refinement, whereby the reduced metal grain size improves mechanical properties, transports reacting elements rapidly to the oxidizing surface, and facilitates the growth of a more adherent scale. This research focused on the effect of substrate grain refinement on the microstructure of its thermally grown oxide, in comparison to the oxide grown on extruded and single crystal NiAl alloys. The oxidation behavior of grain refined materials produced by via sputter deposition, ball milling, and cryomilling was found to vary significantly. Sputter deposition was shown to significantly increase the parabolic steady state oxidation rate constant, while decreasing the length of transient oxidation. Ball milling did not result in an increase in oxidation rate, but did show increased interfacial void formation as a result of the Al2O3 dispersions incorporated during the milling process. Last, cryomilling resulted in an increase in steady state oxidation rate and increased interfacial void formation that was correlated to AlN dispersions incorporated during milling. All three grain refinement methods were found to decrease the oxide grain size approximately three-fold in comparison with the oxide grown on extruded NiAl, though a consistent relationship between oxide grain size and steady state oxidation rate was not observed. This suggests that microstructural features other than substrate and oxide grain size dominate the oxidation behavior.
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    Correlation between heat input and residual stresses from friction stir welding of AA5052 plate
    (University of Alabama Libraries, 2018) Zhu, Ning; Brewer, Luke N.; University of Alabama Tuscaloosa
    This thesis investigates the connections between friction stir welding (FSW) parameters, simple energy/heat input metrics, and the resultant residual stresses on AA5052-H32 plates. A range of weldments were produced with different tool rotational and traverse speeds to produce the same values of the pseudo heat index (PHI). Average residual stresses inside the stir zone and peak residual stress in the thermo-mechanically affected zone were systematically recorded using laboratory x-ray diffraction. In addition, thermal cycles on the advancing side of the welds were collected and analyzed for comparison with the predictions of heat input based upon FSW parameters. Based upon these results, the PHI is not a good predictor of the peak residual stress for welding conditions which produced sound welds. Increasing traverse speed, V, with fixed rotational speed does increase the residual stresses inside the stir zone. The data in this thesis suggests that there is a complex relationship between frictional heating and mechanical stirring of the material. As a result, there is a rotational speed, which requires minimum torque during welding.